絞り込み

16643

広告

Simultaneous Quantitative Detection of 10 Phthalates in PVC Children's Toys by HPLC-PDA.

著者 Akkbik M , Turksoy VA , Koçoğlu S
Toxicol Mech Methods.2019 Jul 31 ; ():1-19.
この記事をPubMed上で見るPubMedで表示
この記事をGoogle翻訳上で見る Google翻訳で開く

スターを付ける スターを付ける     (9view , 0users)

Full Text Sources

method has been developed and validated for the identification and quantification of ten phthalates; in children's PVC toys. The phthalates were extracted from PVC toy sample using ultrasonic extraction with methanol. Quantification analysis was achieved by gradient elution mode using reversed phase ODS-4 C column with PAD detection at 226 nm. The method has been validated for (BBP, DOP, DINP and DIDP) and (DEP, DAP, DBP, DCHP, DHP and DEHP) in the concentration range of 1-100 and 2-200 mg L, respectively. The accuracy determined as recovery were 82.85-107.40% with RSD values at 0.8-4.2%. The limits of detection for (DEP, DAP, BBP, DBP, DCHP, DHP, DEHP, DOP, DINP and DIDP) were 0.02, 0.04, 0.01, 0.03, 0.02, 0.03, 0.03, 0.01, 0.08 and 0.10 mg L, respectively.
PMID: 31364916 [PubMed - as supplied by publisher]
印刷用ページを開く Endnote用テキストダウンロード